Table 2. Mobile phase condition of HPLC

Time (min) A% (0.1% phosphoric acid in water) B% (acetonitrile)
0 95 5
5 95 5
15 90 10
25 87 13
30 85 15
35 83 17
55 80 20
75 70 30
85 40 60
90 10 90
93 10 90
95 95 5
100 95 5